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[PubMed: 25932639] [PubMed: 36455010] Document what matters Lot number and COA reference Receipt date and initial storage condition Aliquoting date(s) and storage location Freeze-thaw count (if relevant) Any observed changes (color, clumping, unexpected assay drift) Practical do this first checklist Store lyophilized peptides at -20C or below in a dry, temperature-stable environment avoid frost-free freezers

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