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J Exp Bot 53(372):12271236 Wonisch W, Kohlwein SD, Schaur J, Tatzber F, Guttenberger H, Zarkovic N, Winkler R, Esterbauer H (1998) Treatment of the budding yeast Saccharomyces cerevisiae with the lipid peroxidation product 4-HNE provokes a temporary cell cycle arrest in G1 phase

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HPLC separates the components of a sample and measures what percentage is actually the target peptide versus impurities

Reviews of this research (including work published in the Indian Journal of Dermatology, Venereology and Leprology ) consistently describe results as inconsistent between studies and dependent on continued use, not permanent once you stop